3.2.2.2. Backscattered Electron Imaging

The electron beam can be rastered across the sample by the deflection coils to produce a BSE image that displays variations in average atomic number, Z. The BSE detector system for the MBX microprobe consists of four semiconductors (PN junctions) located at the bottom of the column at a 40º take-off angle (Figure 3.2.2.2a). When backscattered electrons strike these semiconductors a current flows. The size of the current (signal) is proportional to the number of electrons hitting the PN junctions. The BSE detectors are sensitive to light and cannot be used when the sample illumination is on.

View of the bottom of the electron column.

Figure 3.2.2.2a. Bottom of the MBX electron column. The SEM detector is the large brass assembly on the right. The BSE outputs run through the assembly in the middle left with two large bolts. The BSE detectors are located at 90o intervals around the opening for the electron beam (center) on the chrome-colored ring. BSE electronics are housed outside the column (Figure 3.2.2.2b).
Figure 3.2.2.2b. BSE electronics located between spectrometers 2 and 3.

BSE electronics.

The spatial resolution of BSE images is poor (at best about 0.1 μm) because BSE are produced from the entire upper half of the interaction volume; however, BSE provide valuable information because of their sensitivity to atomic number variations (Figures 3.2.2.2c,d,e). BSE images are displayed on the MAC 3 computer and acquired using the NIH imaging software.

 Backscatted image of exsolution of cpx in large opx grain.

Figure 3.2.2.2c. Backscattered electron image of exsolution of orthopyroxene lamellae in large iron-rich meteoritic pigeonitic pyroxene.

Figure 3.2.2.2d. Backscattered electron image (left) of large zoned olivine crystals and glassy matrix with tiny quench crystals. The strong iron enrichment in the rims of the olivine is easily observed in the backscattered image.

Backscatted image of quench crystals nucleated on a quartz grain

Figure 3.2.2.2e. Backscattered electron image (left) of quench crystals nucleated on a partially melted quartz grain. Interstitial material is glass. The false color image (right), generated from the original grayscale image, emphasizes differences.

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Copyright 1997-2003, James H. Wittke

Last update: 01/18/2006 01:47 PM.